GCMS calibration table, sample AD23914, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\LBA.D Vial: 11 Acq On : 17 Oct 2001 11:05 pm Operator: 209 GALOS San^le : lab blk 10/4 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.52 ug/1 51361 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 1,4-Di orobenzene-d4 150 C6C12D4 003855-82-1 50 2 Benz ne, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 27 3 Be: fenamine, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 22 4 !nzene-l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 Abundance Scan 717 (11.626 min): LBA.D (-) m/z 149.90 100.00% 1ii0

5000 115 78 52 I m/z 151.90 64.70% nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1.4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 33.51% 35 n/z-> ' M " '40" ' 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyf-4-nitro- 77 106 1!I2 -p-r-r-p-n-n-p-r TT-p-r 11.20 11.40 U.K) 11.80 12.00 5000- "m/z 78.05 21.72% 51 94 66 TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66885: Benzenamine, 2-methyt-5-nitro- T-r-p-r 77 106 P ' '' 1 • ' ' •T 152 11.20 11.40 11.60 11.80 12.00 “mTz 52.00 15.81%

5000 51 94

T p-m-p-m-T Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11,60 11,80 12.00

LBA.D NP101901.M Tue Oct 23 12:54:02 2001 Page 5

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