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Document / 13 pages

GCMS sample extraction log table, Nov 2001

Machine-extracted title · confidence 85%

Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

NYC-WTC_000068400–000068412

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068411
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\LB.D Vial: 9 Acq On : 2 Nov 2001 10:50 pm Operator: 209 GALOS Sample : 10/12 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.56 ug/1 84051 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenzeii^d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 36 3 Benzenamine, 2-;pfethyl-4-nitro- 152 C7H8N2O2 000099-52-5 22 4 Benzenamine, ^--methyl-5-nitro- 152 C7H8N2O2 _____ 000099-55-8 14 Wjundance / Scan 712 (11.579 min): LB.D {-) 7 m/z 149.90 10^.00% 1!i0

5000 115 78 52 11 20 11.40 11.60 11.80 12.00 38 45 I 63 87 ' ' I I > I ' I ' I'l I I I I . I I . .. 4^ m/z 151.90 _ 58.49% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11 20 11.40 11.60 11.80 12.00 52 m/z 114.90 32.89% 35 ........Y. ..,.,.,,,.,.,,,1,1........... ... nnfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5.6-clichloro- 150 ■n" 115 11 20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 20741%

35 87 I I ' ' I ' ' ' ' I ' ' I ‘ ' I ' ' ' ' I ' ' ' ' I ' ' mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 106 Ite 11 20 11.40 11.60 11.80 12.00 m/z 52.00 14.53%

5000 51 94

66 m/z-> ' ' i ' ' ' ' I ' ' ' ' I 30 40 50 60 70 4^ 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

LB.D NP103001.M Wed Nov 07 13:12:43 2001 Page 6

NYC-WTC_00006841 1

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NYC-WTC_000068411Source: NYC Law Department, mirrored locally

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