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Document / 13 pages

GCMS sample extraction log table, Nov 2001

Machine-extracted title · confidence 85%

Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

NYC-WTC_000068400–000068412

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068410
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\LB.D Vial; 9 Acq On : 2 Nov 2001 10:50 pm Operator: 209 GTkLOS Sample : 10/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.70 1.18 ug/1 177812 1,4-Dichlorobenzene-d4 11.71

Hit# Of 5 Tentative MW MolForm CAS# Qual

1 2-Pentanone, 4-hydpdxy-4-methyl- 116 C6H12O2 000123-42-2 42 2 2-Propanol, 2-methyl- 74 C4H10O 000075-65-0 12 3 Morpholine, 4-m^hyl- 101 C5H11NO 000109-02-4 9 4 5-Hexen-2-one Z 98 C6H10O 000109-49-9 9 Abundance Scan 289 (7.696 min): LB.D (-) Wz 42795 100.00% 40

59 5000

101 ....... .......... 7.40 7.60 7.80 8.00 53,,, 71 + r-|—tH—r-r—p 7' '' ' I m/z 59705 53.59% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 40

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 21.88%

L 15 31 _l , ' I ' ■I 7 -n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62572:2-Propanol, 2-methyl- 50

7.40 7.60 7.80 8.00

JI 5000 m/z 5^705 :19.17% 31 41

2Q ,1 4 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- ' ' ' I ' * ' ' 1 ' ' ' ' I ' ' ' 4|3 7.40 7.60 7.80 8.^ m/z 40.95 8.76%

5000

15 101 27 71

■n^-> JU ' ‘ I ' ' ' ' I ' 10 20 30 40 I7 I I I 'll I I 50 60 70 ' I ' ' ' ' I ' ' ' ' 1 ' ' ' ' I 80 90 100 110 7.40 7.60 7.80 8.00

LB.D NP103001.M Wed Nov 07 13:12:41 2001 Page 5

NYC-WTC_000068410

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NYC-WTC_000068410Source: NYC Law Department, mirrored locally

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