GCMS blank analysis report sample AE12098, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY3102\LB.D Vial: 3 Acq On : 31 May 2002 1:54 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K. L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.07 0.99 ug/1 62666 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 2 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 Butane l-ethoxy­ 102 C6H140 000628-81-9 9 Abundance 7 Scan 330 (8.072 min): LB.D (-) m/z 42.90 100.00% 40

5000 59

101 —PPPTRTTRPT 83 . | 7.80 8.00 8.20 8.40 ‘ ■ i r ■ ■ ■ i ‘ 38 • i 1 ‘ 1 ' 1 1 I • » * > I t ‘ I < ’» • ‘ J ‘ ‘ » I ) * » > * I 1 m/z 59.00 50.13% miz-> 10 20 30 40 * 50 ' 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 —4 014 ro , । i > , r 59 7.80 8.00 8.20 8.40 m/z 101.05 17.84% 27 . 101 miz-> ............. 10 20 30 11 40 50 +49—+ —m—TT 60 70 80 83 90 । 100 110 Abundance

5000 31 #1691:3-Hydroxy-2-pentanone 59

m/ Z h. 7.80 8.00 8.20 8.40 58.00 16.67% 45 15 , 66 $00 —— 73 —— 84 —— 102 ' ' i ■ ‘ ' • i ‘ ‘ i ‘ ‘ ' i ' TTT+ 1 mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- TT I ‘ ‘ 43 7.80 8.00 8.20 8.40 m/ Z 41.00 8.49% 5000

15 101 71

miz~> 27 ------------ 10 20 30 40 50 56 * 60 70 80 I 90 100 110 AA 7.80 8.00 8.20 8.40

LB.D GCMS0531.M Mon Jun 03 09:35:55 2002 Page 1

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