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GCMS calibration table May 31, 2002, DEP Labs

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Calibration data table for GCMS analysis containing internal standards and surrogate compounds dated May 31, 2002.

NYC-WTC_000014853–000014859

Folder label: “GCMS X 5/29/02 A 5/30/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2302\12097.D Vial: 12 Acq On : 23 May 2002 10:59 pm Operator: Morgan Sample : 5/21 bn Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 15:53 2002 Quant Results File :GCM$0520. RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator! J Title : 209 625/TCLP calibration table \ P) Last Update : Fri May 31 15:47:14 2002 y 3 | / Response via : Initial Calibration X 9 / DataAcq Meth : GCMS0520 VN /s

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12 -14 152 535590 40.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 1950428 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.09 164 1058752 40.00 ug/1 0.00 30) Phenanthrene-diO 25.52 188 1389186 40.00 ug/1 0.00 38) Chrysene-dl2 33.58 240 774801 40.00 ug/1 -0.03 44) Perylene-dl2 37.79 264 539904 40.00 ug/1 -0.01 System Monitoring Compounds 28) TCMX 23.23 209 131533 :24. 2 g/L .00 Spiked Amount 40.000 Recovery 61.80% e

Target Compounds Qv< ue 2) N-nitrosodimethylamine 0.00 74 0 N.D 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.84 128 542 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.57 149 569 N.D. 26) 4-Chlorophenylphenylether 23.23 204 456 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.24 168 347 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) HexachlOrobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.58 178 223 N.D. (#) = qualifier out of range (m) = manual integration 12097.D GCMS0520.M Fri May 31 15:53:33 2002 Page 1

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