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GCMS analysis results sample AE12154, June 2002

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Analytical report for sample AE12154 detailing GCMS results and surrogate recovery data from June 6, 2002.

NYC-WTC_000013351–000013359

Folder label: “GCMS X 5/22/02 A 5/25/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY2402\12154.D Vial: 8 Acq On : 24 May 2002 10:26 pm Operator: Morgan Sample : gc/ms scan 5/22 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 11:47 2002 Quant Results File:,GCMS0520 .RES *es Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 11:39:13 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.14 152 527736 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 2115431 40.00 ug/1 -0.01 17) Acenaphthene-diO 21.09 164 1010203 40.00 ug/1 0.00 30) Phenanthrene-diO 25.52 188 1439676 40.00 ug/1 -0.01 38) Chrysene-dl2 33.57 240 735760 40.00 ug/1 -0.04 44) Perylene-dl2 37.79 264 492238 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.23 209 174103 34.29 ug/L 0.00 Spiked Amount 40.000 Recovery 85.72% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.14 146 128 N.D. 5) 1,4-Dichlorobenzene 12.14 146 128 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.56 149 444 N.D. 26) 4-Chlorophenylphenylether 23.23 204 1025 N.D. 2 7) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.23 168 302 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.51 178 727 N.D. (#) = qualifier out of range (m) = manual integration 12154.D GCMS0520.M Tue May 28 11:48:12 2002 Page 1

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