GCMS analysis results sample AE12155, June 2002

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Analytical report for sample AE12155 detailing GCMS results and surrogate recovery data from June 6, 2002.

NYC-WTC_000013360–000013368

Folder label: “GCMS X 5/22/02 A 5/25/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2402\12155.D Vial: 9 Acq On : 24 May 2002 11:26 pm Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 11:58 2002 Quant Results File: GCMS0520.RES *es Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 28 11:39:13 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.14 152 521589 40.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 2052162 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.08 164 975404 40.00 ug/1 0.00 30) Phenanthrene-diO 25.52 188 1382301 40.00 ug/1 -0.01 38) Chrysene-dl2 33.57 240 664208 40.00 ug/1 -0.03 44) Perylene-dl2 37.78 264 428914 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.22 209 173680 35.43 ug/L -0.01 Spiked Amount 40.000 Recovery 88.58% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.15 146 604 N.D. 5) 1,4-Dichlorobenzene 12.15 146 604 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.83 128 276 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.57 149 450 N.D. 26) 4-Chlorophenylphenylether 23.22 204 1104 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.24 168 280 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.52 178 249 N.D. (#) = qualifier out of range (m) = manual integration 12155.D GCMS0520.M Tue May 28 11:58:50 2002 Page 1

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GCMS analysis results sample AE12157, June 2002 · Box DEP Box 15

NYC-WTC_000013378

Gas chromatography-mass spectrometry analysis of sample AE12157 performed on 6/7/02, detecting unknown compounds and 2,4-DDD surrogate at 83% recovery.

1 shared topics · Same agency, volume and box · similarity 0.999