GCMS calibration table May 31, 2002, DEP Labs

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2302\12097.D Vial: 12 Acq On : 23 May 2002 10:59 pm Operator: Morgan Sample : 5/21 bn Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.12 9.22 ug/1 624443 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl - 116 C6H1202 000123-42-2 72 2 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 3 Acetone 58 C3H60 000067-64-1 9 4 3-Hydroxy-2-pentanone________ 102 C5H10O2 003142-66-3 9 Abundance / Scan 335 (8.118 min): 12097.D (-) m/z 42.90 100.00% 43

5000 59 t

101 1 ‘ ' l 1 ‘ ‘ ‘ I ■ ‘ ‘ ‘ I ' ■ ■ ■ I ‘ ‘ ‘ I 7.80 8.00 8.20 8.40 miz-> mp10n)20. 30 38, +53+ 40 50 60 #****——TT — 11" 0 70 80 83 90 100 110 m/z 59.00 49.51% Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 0I141duoa 1a I | I l l I' 59 7.80 8.00 8.20 8.40 m/z 100.95 21.65% 27 101

miz-> ----- 10 20 30 40 +49+ 50 1**44 60 70 83 >-]>*•* 1 1 « 80 90 + 100 110 Abundance #1640: Morpholine, 4-methyl- 43 ■ 1 i 1 • ' ' i ■ ‘ i ■ • 1 ' r 7.80 8.00 8.20 8.40 5000 m/ z 58.00 20.37% 15 101 27 71 11 11 l ■ ■ ‘ ‘ I 56 I 000 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i • ■ ■ ■ i • ■ ■ ■ i 43 7.80 8.00 8.20 8.40 m/z 41.00 6.64% 5000 58 27 ----- li - 1 * iz—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 J

12097.D GCMS0520.M Fri May 31 15:46:48 2002 Page 1

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