GCMS calibration table data, DEP Labs, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3002\11284.D Vial: 11 Acq On : 30 May 2002 11:55 pm Operator: Morgan Sample : re-ext Inst : 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.06 1.25 ug/1 100852 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 74 2 Acetone 58 C3H60 000067-64-1 12 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 5-Hexen - 2 - one 98 C6H10O 000109-49-9 9 Abundance, Scan 329 (8.063 min): 11284.D (-) m/z 42.95 100.00% 43

5000

miz-> ........ ■• i ■ ■ ■ ■ i ' • ■ 1 । 10 .......................‘■. rr' 20 30 40 50 49 60 59

+ ————83—— 70 . I 80 m/z 90 101

100 110 TPi 1 I1 7.801 TTme 8.00 !59.00 L8.20 8.40 48.12% Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ' ‘ I ‘ 1 59 7.80I 8.00 8.20 8.40 m/ z !58.00 18.67%

J 15 31 . 101 | i ------ ' ■ i • ■ ■ ■ i ■ • ■ ■ i ■ 1 1 1 i 1 1*1’1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone 43 ■ • i < • 7.80 8.00 8.20 8.40 5000 m/z 101.05:17.70%

niz—> Abundance 10 201 27 lonnop 30 40

43 1 ' ' I ' ' 50 60 58

। ■ ■ ■ • । 1 ■ ■ ■ । ■ ■ ■ ‘ । ‘ ■ ■ • i • ■ ■ ■ । ■ 70 #1640: Morpholine, 4-methyl- 80 90 100 110

m/z ___ ’*I**’I44* T11 ■ ■ i ■ ■ 7.80 40.90 L 8.00 8.20 8.40 8.75% 5000

15 101 27 71 I -------- -------- 56 I 1 ‘ ' I 1 ' 1 ' 1 1 n/z—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

11284.D GCMS0520.M Fri May 31 11:33:57 2002 Page 1

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