GCMS analysis report sample AE12097, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY3002\12097.D Vial: 16 Acq On : 31 May 2002 4:48 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) «‘** Title : 2(79 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.06 1.00 ug/1 85751 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4 -methyl- 116 C6H1202 000123-42-2 56 2 CH2=CHCH2C (0) OCH3 100 C5H802 003724-55-8 10 3 5-Hexen-2-one 98 C6H10O 000109-49-9 9 4 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 Abundance Scan 329 (8.062 min): 12097.D (-) m/z 43.00 100.00% 43

5000 59

101 —r-r-r-r-p-TT

miz-> m +51++ 10 20 30 40 50 60 I ■ ■ ■ ■ i 1 1 ■ ■ i 70 80 83 ■ ■ i ■ ■ ■ 1 i ‘ • ■ 1 i ■ 90 100 110 m/z 7.801 8.00 8.20 8.40 !59.00 49.53% Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 Pmmmm 59 7.80 8.00 8.20 8.40 m/z 101.05 19.56% 27 101

miz-> 10 20 30 I i T +49 + 40 50 60 I p • ■ ■ p ■ ■ ITT* । । । 70 80 83 90 + 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43

" t. 7.80 8.00 8.20 8.40 5000

38,4 10****■ 58 72 100 niz->_____ 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205:5-Hexen-2-one -r-r-p-r 43 7.80 8.00 8.20 8.40 m/z 40.90 ‘ 6.99% 5000

55 15 27 m/z—> ......... I .......... 1.......... 38,. 10 20 30 40 1IT50 83 98 —r ■ • p • • • p • • • p’> • • p • ■ I P । । । P 50 60 70 80 90 100 110 AL 7.80 8.00 8.20 8.40

12097.D GCMS0520.M Fri May 31 11:35:10 2002 Page 1

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