GCMS analysis report sample AE12097, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3002\12097.D Vial: 16 Acq On : 31 May 2002 4:48 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) . Title : 2d9 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 25.57 0.41 ug/1 50518 Phenanthrene-dl0 25.43 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene -d10- 2 Phenanthrene-dl 3 Naphthal ene, 1,7- dimethoxy- 79 188 C14D10 188 C14D10 188 C12H1202 001719-06-8(91 001517-22-2 86 005309-18-2 36 4 Pentacycyo[8,4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 36 Abundance Scan 2236 (25.569 min): 12097.D (-) m/z 188.10 100.00% 118

5000

80 94 ■ i 1 ■ ■ ■ i ■ ■ 1 I ■ 1 1 1 i ' 1 1 ' i 1 25.20 25.40 25.60 25.80 miz-> 49 66 i-rr| »> i ?j i-ri • 11,1, ( in i 40 50 60 70 80 m ...... , .................................... 146 Puummmuun* 90 100 110 120 130 140 150 160 170 180 190 . 158 ] m/z 94.00 17.16% Abundance #19957: Anthracene-d1 0- 118

5000 -------- 25.20 25.40 25.60 25.80 m/z 189.10 15.83% 66 80 94 160

miz-> “ i111' i ■" ■ i ■" ' i" " i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 -H Abundance

5000 #19958: Phenanthrene-d10 118 TT u 25.20 25.40 25.60 25.80 m/z 184.10 Tl ITIII

14.61%

80 94 160

miz—> 40 66 mPPH ll mmpmmgl] 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ‘tE1 —

Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 108 25.20 25.40 25.60 25.80 " ‘ ' m/z 80.00 14.07% 5000 102 115 145

51 63 75 94 . 130. .,..1... ....... Hp i........ ‘110137 m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80

12097.D GCMS0520.M Fri May 31 11:35:11 2002 Page 2

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