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Document / 11 pages

GCMS analysis results for sample AE12576, June 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12576 conducted on June 6, 2002.

NYC-WTC_000014923–000014933

Folder label: “GCMS X 5/29/02 A 5/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY3102\12576.D Vial: 10 Acq On : 31 May 2002 8:51 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531 .M (RTE Integrator) Title : 20*9 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.57 0.51 ug/1 50134 Phenanthrene-dl0 25.42 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene -d10- 188 C14D10 001719-06-8 91 2 Phenant hrere-d1 64 188 C14D10 001517-22-2 50 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 4 Pentacyc [8.4.0.0(3,7) .0 (4,14) .0(6 188 C14H20 000000-00-0 36 Abundance Scan 2236 (25.571 min): 12576.D (-) m/z 188.10 100.00% 1118

5000

80 94 25.20 25.40 25.60 25.80 26.00 160 , . .... 421 .... 1... ■ "i■■•■i1 ■ ■' i ■ -r-■ hL 1111 * 11'11111111 LB8 m/z 189.10 17.22% mlz->40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 1118

5000 TIE ■ ■ i ■ ■ ■ ■ i ■ 25.20 25.40 25.60 25.80 26.00 m/z 94.05 15.67% 80 94 160 ................... 66 miz-> ■ ■ i * ।■ i ■ M1 111 ip 11111111111 > 11111 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ...... IJ.... Abundance #19958: Phenanthrene-d10 1(18

25.20 25.40 25.60 25.80 26.00 5000 m/z 79.95 13.48%

80 94 160 66 mfz-> - 0100 n >. । ।. 11111 11 “ '111 ‘ ' I' ■ ■ ‘ i ‘ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ..... Il.. Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 25.20 25.40 25.60 25.80 26.00 m/z 184.05 13.43%

5000 102 115 145

m/z—> 51 63 ’1000310031 7.A4L15 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25:20 25.40 25.60 25.80 26.00

12576.D GCMS0531.M Mon Jun 03 09:35:20 2002 Page 3

NYC-WTC_000014932

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NYC-WTC_000014932Source: NYC Law Department, mirrored locally

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