GCMS unknowns report for sample AE12281, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2902\12281.D Vial: 22 Acq On : 30 May 2002 7:58 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

25.57 0.44 ug/1 47963 Phenanthrene-dl0 25.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene - 188 C14D10 001719-06-8 87 2 Phenanthren -41059 188 C14D10 001517-22-2 78 3 Pentacyclol 8.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 36 4 Cyclohexanone, phenylhydrazone 188 C12H16N2: _____ 000946-82-7 33 Abundance Scan 2236 (25.570 min): 12281 .D (-) m/z 188.10 100.00% 118

5000

80 94 160 . i 25.20 25.40 25.60 25.80 26.00 42 52 66 132 —PT HH I ‘‘ ‘ I 'I1,“I — m/z 189.10 17.32% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 25.20 25.40 25.60 25.80 26.00 m/z 94.00 13.54%

mlz-> Abundance „5 94 1 ‘ i11 •' i *1' * r 1 * ’ i1 * ‘11'1 •111 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #19958: Phenanthrene-d10 118 ■ i • ■ ■ ■ i ■ ri ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 25.20 25.40 25.60 25.80 26.00 5000 m/z 80.05 12.89%

160 66 —mmpo —— I " ‘' I "'11 ‘ ' I m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19959: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11)]tetradecane 1)18 25.20 25.40 25.60 25.80 26.00 m/z 184.10 12.27%

5000 79 92 117 106 131 145 159 173 ' ■ i ■ ■" i ■" ■ i ■ ■ ■ • i" “ I ■ “ ‘T HH++ L'j. ■ ■»i')'. ■ ।. m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80 26.00

12281.D GCMS0528.M Thu May 30 10:39:20 2002 Page 3

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