GCMS analysis report, sample AE04417, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\4417.D Vial: 8 Acq On : 21 Mar 2002 6:10 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.22 ug/1 44194 Phenanthrene-dl0 25.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dl0/ 77 188 C14D10 001719-06-8 87 2 1,4-Naphthalenedione, 2-hydroxy-3-m 188 C11H803 000483-55-6 42 3 Cyclohexanone', phenylhydrazone 188 C12H16N2 000946-82-7 38 4 Phenanthrene/diO 188 C14D10 __ 001517-22-2 37 Abundance C Scan 2260 (25.796 min): 4417 b() m/z 188.10 100.00% 188

5000

80 94 . 160 25.40 25.60 25.80 26.00 26.20 40 54 66 ? .I miz-> mhmmmmmmmmmm l 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 189.10 20.90% Abundance #19957: Anthracene-d10- 188

5000 25.40 25.60 25.80 26.00 26.20 80 94 m/z 94.00 14.00% 66 160 mTTTTT 1-mnpmmmmp miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance *60174: 1.4-Naphthalenea we 2 wdroxy-2-metyl 188

25.40 25.60 25.80 26.00 26.20 5000 m/z 184.10 10.27%

50 77 105 131 160 00 । > i i i । i ' i । i i > i । i i t »f i 11 . ।m . । i i 115 । । । . i . । । 1001.1m00-—-u—OOum37 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19927: Cyclohexanone, phenylhydrazone 188 25.40 25.60 25.80 26.00 26.20 93 m/z 80.05 10.18% 5000- 65 77 106 145 | 120 132 | 159 170 “ i ■ ■ ■' । ■11 ■ i ‘ ■ i • ■" i ■1 u ‘ I" “ I “1 ‘ i1 “' i11" i “ “'i “ ■ • i ■ “ ‘ i “ T’T m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

4417.D GCMS0308.M Fri Mar 22 09:39:07 2002 Page 3

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