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GCMS analysis results for sample AE02597, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02597 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005281–000005290

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005288
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR0102\2597.D Vial: 7 Acq On : 1 Mar 2002 2:15 pm Operator: Sample : gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.27 ug/1 30901 Phenanthrene-dl0 25.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene -d10- 775 188 C14D10 001719-06-8 72 2 Phenanthrene-d10 188 C14D10 001517-22-2 56 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 4 - (4-Tolyl) -3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 37 Abundance ■ Scan 2267 (25.851 min): 2597.D () m/z 188.10100.00% 185

5000

66 80 94 '56

m/z-> 44 -L -80 l mmpl — m/z 11 1 11 1 ' 1 1 1 40 50 60 70 IT 90100 110 120 130 140 150 160 170 180 190b 25.60 25.80 26.00 26.20 80.00 20.18% Abundance #19957: Anthracene-d10- 183

....... .............. 5000 25.60 25.80 26.00 26.20 m/z 155.95 15.92% 66 80 94 160 " i " ” i1 " 1111'1111 ‘‘11 ‘ 1 1 | 1 1 1 | ■ 1 1 1 ..................... . । > > > । । i rr । i i i । । i i । i' । । । m/z—> Abundance 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190

188 1........ 25.60 25.80 26.00 26.20 5000 m/ z 66.05 14.91%

80 94 160 66 '11 1'' ' i'1 ■ ‘ 11''' r '1 11 '' ■ ■ ir 1'' i ''1' i1 1 ■' iri 1' 111111 11 1 11''1 11 111111'11 | 111111' m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ----- Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 25.60 25.80 26.00 26.20 m/z 94.00 14.73% 5000 115 145 102 ..................................................... 51 63 75 94 130 158 । '' i " ' ' i " " !1111 11' '''11 " " 111111 "I111 >11 1 1'1 '' i " 1 111''11'11 1111 1 TTI m/z~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2597.D GCMS0208.M Mon Mar 04 11:41:24 2002 Page 2

NYC-WTC_000005288

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NYC-WTC_000005288Source: NYC Law Department, mirrored locally

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