GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31552.D Vial: 15 Acq On : 19 Jan 2002 5:15 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

24.91 0.23 ug/1 66741 Phenanthrene-dl0 24.77

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene -ai0- 59 188 C14D10 001719-06-8 90 2 Phenanthrene-dl0 188 C14D10 001517-22-2 90 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 50 4 - (4-Tolyl) -3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 47 Abundance - Scan 2164 (24.914 min): 31552.D(-) m/z 188.10 100.00% 188

5000 T TTT _ . 80 94 24.60 24.80 25.00 25.20 -Hp 42 52 66 146 160 ■ ■ । ■1 ■11"1111'1 irh 111111।. m/z 184.10 16.77% m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 ‘ 1 | । i r • p ’T i । i i i i |"i i i i |' 24.60 24.80 25.00 25.20 80 94 m/z 189.10 14.94% 66 160 mP—mmmpmmpmgmp m/z-> " i ■ ■ ■ • i ■ • ■ • i ■ ■ “ i ■ • 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d 0 188

24*60 24.80 25.00 25.20 ' 5000 m/z 94.00 13.89%

66 80 94 160 1PPILTLWTWLTTIT ‘l‘ ‘‘I‘‘‘*1*11*1‘41/1+4**1***‘1****1/**1**/11* m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- 188 24.60 24.80 25.00 25.20 ' ‘ 173 m/ z 8.0.05 13.37% 145 5000 102 114 130 ■ ■ ।।u 1 ■ ।। 76 । ■11 9 ‘ ■ ■ ■ । Tmmamugtt ,17.. — 1' i ■ " ' i'' " i ■1 ■ ■ i " - 24.60 24.80 25.00 25.20 ~ miz->30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190

31552.D GCMS0103.M Wed Feb 06 15:42:47 2002 Page 2

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