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GCMS analysis results for sample AD31402, Feb 11, 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31402 conducted on February 11, 2002.

NYC-WTC_000016341–000016351

Folder label: “GCMS X 12/28/01 A 1/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31402.D Vial: 19 Acq On : 17 Jan 2002 5:13 am Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

24.92 0.25 ug/1 73077 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene 0- A ‘ 188 C14D10 001719-06-8 83 2 Phenanthre: diO 188 C14D10 001517-22-2 59 3 Naphthalen 1,7 -dimethoxy- 188 C12H1202 005309-18-2 38 4 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 _ 005603-22-5 37 Abundance Scan 2165 (24.917 mln): 31402.D (-) . ....... . ’ ......... / z 188 710 100.00% 118

5000 94 40 52 64 132 146 158 I I 24.60 24.80 25.00 25.20 1,1 mmapp -mh m/z 94.00 22.40% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 T-CJ I l f 1 I T I | I J I I | I I | ! | 24.60 24.80 25.00 25.20 m/z 189.10 17.11 66 80 94 Tmpo*—ann)"mmnmm*ummOmmpm 160 I. miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19058 Phepanthrene-g10 188

24.60 24.80 25.00 25.20 ' ' ' 5000 m/z 184.10 11.73%

66 80 94 160 । miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ........... ..................................... Abundance #19913: Naphthalene, 1,7-dimethoxy- 1 ' I ' ‘ ‘ I ‘ ‘ 1 ' 1 1 1 1 ‘ I 1 1 ' ' I 173 188 24.60 24.80 25.00 25.20 m/ z 80.05 10.86% 5000 102 115 145 51 63 75 94 130 158 .. 11.... f.... ।.... ।. ।11,1 ■. । mMHmm 11 ‘“ I' ■ ■11 “ ■ ■ i ■ ]__ hs 24*60 24.80 25.00 25.20 ‘ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190

31402.D GCMS0103.M Thu Feb 07 12:35:37 2002 Page 2

NYC-WTC_000016349

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NYC-WTC_000016349Source: NYC Law Department, mirrored locally

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