GCMS analysis summary, sample AD31403, Feb 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31403.D Vial: 12 Acq On : 15 Jan 2002 9:43 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

24.93 0.23 ug/1 60421 Phenanthrene-dl0 24.77

Hit# of 5 Tent at. ID MW MolForm CAS# Qual

1 Anthracene-d10- / 188 C14D10 001719-06-8 83 2 Phenanthrene-diO 188 C14D10 001517-22-2 83 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 50 4 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 47 Abundance Scan 2166 (24.928min): 31403.D (-) m/ z 188.10° 100.00% 118

5000 80 94 DnnnmnnmmummDTTT 41 52 6g I TWHmp ■ 11 ■' ■ rHT «2 t।t... u i... 11m— m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 . 24.60 24.80 25.00 25.20 m/z 80.05 20.46% Abundance #19957: Anthracene-d 10- 188

5000 24.60 24.80 25.00 25.20 80 94 -(go m/z 189.00 16.62% 66 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188 24.60 24.80 25.00 25.20 ' ' ‘ 5000 m/z 94.00 14.55%

. 66 80 94 160

m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 108 24.60 24.80 25.00 25.20 m/z 184.10 13.83% 5000 115 145 102 75 94 130 ‘ 1PTTT Tp TH I " 1' I'1 l' 158 1 ITT I' " 11' i'1' ‘ i ■■।■1■।1'1■।1■11। m!z~> 30 40 50 60 70 80.90100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20

31403.D GCMS1126.M Mon Feb 04 15:11:42 2002 Page 4

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