GCMS analysis results for sample AD29932, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC18O1\29962.D Vial: 11 Acq On 19 Dec 2001 1:51 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

25.12 0.32 ug/1 114660 Phenanthrene-dl0 24.97

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 58 2 Phenanthrene-d10 188 C14D10 001517-22-2 53 3 1,4-Naphthalenedione, 2-hydroxy-3-m 188 C11H803 000483-55-6 40 4 Benzene, 1-(1-cyclohexen-l-yl)-4-me 188 C13H160 _______ 020758-60-5 23 Abundance Scan 2187 (25.121 min): 29962.D (-) m/z 181710 100.00% 188

5000- 80 ............ / <.............................. 92 160

1190.198...... 136 146— l 24.80 25.00 25.20 25.40 n-p- V’T m/ z 80.05 27.72% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 'Abundance #19957: Anthracene-d10- 188

5000- ) I • • ■ ■ I 24.80 25.00 25.20 25.40

.... 66.8 4 94 l 160 — m/z 189.10 21.81%

m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

24.80 25.00 25.20 25.40 5000- m/z 160.05 20.22% 80 94 160 | 66 | J .............................. 11.............. l ■i•>■•i•• ■ • i ■ ■ i ■ ■ ■ ■ i • ■ • ■ I • । ‘ ■ ■ ■ । TTTTIITT ■ I | । । 11 i 11 n 11 i i i i । । । m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69174: 1,4-Naphthalenedione, 2-hydroxy-3-methyl- ) 188 24.80 25.00 25.20 25.40

.L m/z 92.00 19.58% 5000

77 160 105 131

m/z—> - 50 ■p-rTTp-nil I | I ! "‘I’ITTTT +115, ' I " " I ' ' TrT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 L 24.80 25.0 25.20 25.40

29962.D GCMS1126.M Tue Jan 15 15:27:50 2002 Page 4

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