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GCMS analysis results for sample AD30013, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report documenting analysis of sample AD30013 conducted on January 28, 2002.

NYC-WTC_000037255–000037268

Folder label: “GCMS X 12/11/01 A 12/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\30013.D Vial: 8 Acq On : 18 Dec 2001 10:55 pm Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Anthracene-d10- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

24.97 18.01 ug/1 6216790 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 96 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 3 Benzene, 1-(1-cyclohexen-l-yl)-4-me 188 C13H160 020758-60-5 36 4 ^ntacyclo[8.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 ____ 000000-00-0 36 Abundance Scan 2171 (24.972 min): 30013.D (-) m/z 188.10 100.00% 188

5000

................... - 80 42 52 66 94 . । 102110118 132 146 160 Hi 1 170 180 24.60 24.80 25.00 25.20 25.40 ■ I'' ■ ■ l'' ■' THT 1111111111111 1111 > > 111111 > 11111 T T T 111111111TTTT ■, 11 ■ । । HTT T T T TT m/z 187.10 17.15% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 1" 24.60 24.80 25.00 25.20 25.40 80 94 m/z 80.0,5 15.55% | ........................... 66 160

m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ... I...... Abundance #19958. Phenanthrene-d10 188 i ■ i • ■ ■ ■ i II 24.60 24.80 25.00 25.20 25.40 5000 m/z 189.10 14.71% 80 94 160 66 1! ■ i • * • • r ■ • ■ l' • ■ • i • • ’ • i • i ■ ■' • i i1 " 11 I ■ > > 11. ■ I 11 " I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19943: Benzene. 1-(1-cyclohexen-1-yl)-4-methoxy- I 188 24,60 24.80 25.00 25.20 25.40 m/z 94.0,0 14.65% 5000 160

121129 1f5 173

m/z—> ' I " " r ''' i1 ■■' i' TTTTIT " i' 30 40 50 60 70 80 TT i ■ ■ ‘11 1... .. ... ."I'" • l " 11'' •' I 90 100 110 120 130140 150 160 170 180 190 _...... 11..... 24.60 24.80 25.00 25.20 25.40

30013.D GCMS1126.M Tue Jan 15 15:34:31 2002 Page 4

NYC-WTC_000037265

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NYC-WTC_000037265Source: NYC Law Department, mirrored locally

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