GCMS analysis results for sample AD30011, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30012.D Vial: 9 Acq On : 18 Dec 2001 11:54 pm Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

25.12 0.31 ug/1 106564 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 001719-06-8 80 188 C14D10 2 Phenanthrene-d10 001517-22-2 72 188 C14D10 3 3M-Pyrazol-3-one, 2,4-dihydro-4,4-d 188 C11H12N2O 017694-06-3 53

S 4/1,4-Naphthalenedione, 2-hydroxy-3-m 188 C11H803 Abundance Scan 2187 (25.123 min): 30012.D (-) 000483-55-6 36 m/z 188.10 100.00% 188

5000 ) 42 — RR 78 94 160 24.80 25.00 25.20 25.40

m/z-> T‘ — 55.66 .. - 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 77.95 13.64% Abundance #19957: Anthracene-d10- 188

5000 24.80 25.00 25.20 25.40 80 94 m/z 94.00 13.14% 160 m/z-> 30 .......................... 66 40 50 A 70 l I'''' I — 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 ............ /................................. 24.80 25.00 25.20 25.40 5000 m/z 160.05 12.25%

RR 80 94 160 ............. 66....‘T‘‘ T"TETTTTEEOETETTTTTTT"TT ‘‘VUi ..... .......................... ‘TITTTTTTTT‘ ‘I‘ i .........I ITETTTUEITTTCTTITITTT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19871: 3H-Pyrazol-3-one, 2.4-dihydro-4,4-dimethyl-2-phenyl- .. 4... 188 24.80 25.00 25.20 25.40 55 m/z 184.10 11.33% 77 5000

160 64 r — ........ 9145 J 119 132 173 ■' r ■ • ■ r ' T’T L 119.8 T-T-T-j-, . , , f > ■ i • ■ ■ ■ । ■ । m/z--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.80 25.00 25.20 25.40

30012.D GCMS1126.M Tue Jan 15 15:32:46 2002 Page 5

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