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GCMS analysis results for sample AD30013, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD30013 conducted on January 28, 2002.

NYC-WTC_000037255–000037268

Folder label: “GCMS X 12/11/01 A 12/18/01

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Scanned page image, NYC-WTC_000037264
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30013.D vial: 8 Acq On : 18 Dec 2001 10:55 pm Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.68 ug/1 171428 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 17(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol,8,3 ‘ -oxybis- 162 C8H18O3 054305-61-2 50 3 2-Propanol, l,l'-oxybis- 134 C6H14O3 000110-98-5 40 4 Ethane<l 1,y 2-diethoxy- 118 C6H14O2 000629-14-1 38 'Abundance Scan 696 (11.431 min): 30013.D (-) m/z 59.05 100.00% 59

5000

-51 45

' 460 + 73

85 103

1 M 11.20 11.40 11.60 11.80

k m/z 45.05 46.95% mlz-> 20 30 40 50 70 80 90 100 110 120 130 140 'Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy)- 59

5000 45 103 11.20 11.40 11.60 11.80 73 31 m/z 103.0 35.67% । 130 m/z--> —20PPP 30 40 4 ' —T 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3'-oxybiS- 59 , —PPP — — , r 11.20 11.40 11.60 11.80 5000- 31 45 m/z 73.00 8.73% 103

I m/z-> Abundance 20 30 40 4 50 60 70 80 90 100 #6087: 2-Propanol, 1,1’-oxybis- 59 110 120 134 130 140 N 11.20 11.40 11.60 11.80 11 I ’ '

NA m/ z 41.05 21.86% 31 5000 - 45 103

m/z-> •20. 30,. 40I ‘II 50 1. 72.. 82 60 70 80 90 100 110 120 130 140 TAf "I ■ ■ ■ l ■ ■ ■ ■ l ' • ■ ■ l ■ ■ ■ 11.20 11.40 11.60 11.80

30013.D GCMS1126.M Tue Jan 15 15:34:26 2002 Page 3

NYC-WTC_000037264

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NYC-WTC_000037264Source: NYC Law Department, mirrored locally

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