GCMS analysis results for sample AD30014, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30014.D Vial: 13 Acq On 19 Dec 2001 3:48 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.63 ug/1 167150 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1 2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2 -Propanol,1 ,11-oxybis- 134 C6H14O3 000110-98-5 56 3 Ether 74 C4H10O 000060-29-7 42 4 2-Buta: 1, 3,3'-oxybis- 162 C8H18O3 054305-61-2 42 Abundance । Scan 696 (11.435 min): 30014.D (-) m/z 59.05 100.00% 59

I

i 5000

m/z-> TIPI 39, 20 । I I I । . । 30 40 45

50 H ( 60 H 70 73

TI—" 1 1 1 1 80 85 90 94 103

100 110 120 130 m/ z N TIT 11.20 11.40 11.60 11.80 44.95 52.40% Abundance #9238: 2-Propanol, l-(2-methoxy-1 -methylethoxy)- । 59

5000 45 103 11.20 11.40 11.60 11.80 73 31 m/z 103.05 31.75% ‘ i ■ ■ ■ p ■ 1 ■ p ■ ■ ' p ' । III 130 mz-s 20 30 40 ■50 60 70 80 90 100 110 120 130 Abundance #6087: 2-Propanol, 1,1’-oxybis- 59

31 11.20 11.40 11.60 11.80 5000 45 m/z 41.05 27.46%

m/z-> Abundance 20 .L 72 I 89 103

■ P ' l p • • • ' p ■ • ' p ■ ■ ' I • • < ■ p ■ ' • p ■ ' ■ P ' • P . . . . I....... . । । | । ' 30 31 40 50 60 70 80 #62576: Ether 90 100 110 120 130

m/z NJ 11.20 11.40 11.60 11.80 73.00 7.14% 59 5000 45 74

। i ' I ' ' ' ' I ' ' ‘ ' I ' 1 1 ' I 1 1 1 'O' 'lip T-T-j-r-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 11.20 11.40 11.60 11.80

30014.D GCMS1126.M Tue Jan 15 15:36:17 2002 Page 4

NYC-WTC_000037311