GCMS analysis results for sample AD29962, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30011.D Vial: 14 Acq On : 19 Dec 2001 4:47 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.36 0.35 ug/1 77848 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, a, 1'-[(1-methyl-l,2-eth 192 C9H20O4 001638-16-0 53 3 2 - Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance "Scan 688 (11.362 min): 30011.D (-) m/ z 59.05 100.00% 59

m/z-> 5000-

20 30 39 il 40 45

. , .................... . , . , TT 1 ■ ■ i ■ '86 50 60 70 73

80 । ' 1 I ' 1 ' ■ i*' ' ' । । । । । । | i । । । । I । 90 100 103

110 120 130 11.00 11.20 11.40 11.60 m/ z N 45.05 52.25% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000- 103 •T 45 11.00 11.20 11.40 11.60 73 31 m/ z 41.05 32.06%

NA 130 m/z-> 20 ' i ' ' ' ' T ------ 30 40 50 60 70 r...... —PPT । 80 90 . — 100 110 120 130 Abundance #20630: 2-Propanol, 1.1-[(1-methyl-1 .2-ethanediy!)bis(oxy) 59 I A MMMMP 11.00 — 11.20 11,40 11.60 5000 m/z 103.05, 30.13% 31 45 103 i 39 | 73 i 117_______ ' I ' ' 4. | . . . , । . . . . । , . . . | , . , . । . I I I | I I I > | I I TCIdu. I j < < II I I I I , I , , m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087: 2-Propanol, 1,1‘-oxybis- 59 11,00 11,20 11.40 11,60 m/z 73.00 25.87%

, AJ 31 5000 45 103 - 89 72 TIT----- +H— • i 1 ' ' ■ i 1 1 1 1 I 1 1 1 1 1 I m/z-> 20 30 40 50 I60 70 80 90 100 110 120 130 11.00 11.20 11 40 11.60

30011.D GCMS1126.M Tue Jan 15 15:31:03 2002 Page 3

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