GCMS analysis results for sample AD29962, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\30011.D Vial: 14 Acq On : 19 Dec 2001 4:47 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.74 1.11 ug/1 248006 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, ,1,1- trichloro- 160 C3H3C130 000918-00-3 38 2 2 -Nonanone, 9-[(tetrahydro-2H-pyran 242 C14H2603 054699-41-1 9 3 Pentanoic—acid, 2,2-dimethyl-, 1,2, 428 C24H44O6 057346-62-0 7 4 Cyclopentanol , 2-methyl-, acetate, 142 C8H14O2 040991-94-4 7 Abundance Scan 293 (7.736 min): 30011.D (-) m/ z 4 3.05 100.00% 43

5000-

35 .,51 59 82,88 97_ 117 125 7.40 V I • । । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ • • । 7.60 7.80 8.00

R′ . । .... । TTTTT TT t 1 T ■ ■1 11 1 '' ■ i ■ ■ ' 1 i h ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ ■ ''' i ' ' ' ' i ■ ■ ■ ■ i • m/ z 59.05 8.56% 10 20 30 40 50 60 70 80 90 100 110 120 130 140 (Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 - AA4 +44 7.40 7.60 7.80 8.00 15 m/z 124.85 6.59% ...... | 35 85 97 117 125 1 1 i ■ ■ ■ 'll ' ’ ' I TTn m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #32337: 2-Nonanone, 9-[(tetratiydro-2H-pyran-2-yl)oxy)- 43

7.40 7.60 7.80 8.00 85 5000 - 58 m/z 81.75 5.27%

71 101 । l |! —........ 141 TIT ■ I 1 1 ’ ■ i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #55792: Pentanoic acid, 2,2-dimethyl-, 1,2,3-propanetriyl e i ■ ■ ■ ■ i 43 85 7.40 7.60 7.80 8.00 m/ Z 96.85 5.08% 5000 74 57 27

m/z-> ............ —........... — 10 20 30 40 50 il 60 70 80 1 101 • • i • ■ ............... । 90 100 110 120 130 140 .............. ............................ ‘ ' i • ■ l ■ ■ ■ ' I ■ ■ ■ • ........................................ I 7.40 7.60 7.80 8.00

30011 .D GCMS1126.M Tue Jan 15 15:30:59 2002 Page 2

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