GCMS analysis results for sample AD29962, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\30011.D Vial: 14 Acq On : 19 Dec 2001 4:47 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number . 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.80 ug/1 853569 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tent ve ID MW MolForm CAS# Qual

1 N-Ethylformami de 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 4 Pentane , 3-methoxy- 102 C6H140 036839-67-5 9 Abundance ' Scan 278 (7,598 min): 30011 D (-) m/z 73.00 ’100.00% 73

5000- 43 7.20 7.40 7.60 7.80 8.00 0 ■ ■ i • ' ■ ' i ■ ■ ' ■ i 35 , |, | 49 55 TIGBddttdnn/n ‘Iil ■ 67, 1 |.......... 87............ 103...................... ■ 1 i ■ m/z 43.05 28.68% m/z-> 10 20 30 40 50 60 70 80 90 100 11i 120 Abundance #292: N-Ethylformamide 30 73

5000 1 i ■ ■ • ■ i

58 7.20 7.40 7.60 7.80 8.00 44 m/z 41.0.0 10.52%

m/z-> 10 5 20 30 — । — 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5.5,5-trichloro-2,2-dimet 73 FIT 1 ( TTTmummrrir 7.20 7.40 7.60 7.80 8.00 5000 m/ z 45.0.5 10.43% 45 36 55 67 ................................. 109 115 ' ' i ' ' ' ■ i ' ' ' ■ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.78% 5000

45 |15 88 | 53 59 ———-mmuor * TGnnnnOOBIOBBntIn m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

30011.D GCMS1126.M Tue Jan 15 15:30:54 2002 Page 1

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