GCMS analysis results for sample AD30015, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30015.D Vial: 12 Acq On 19 Dec 2001 2:50 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.64 ug/1 177393 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 17 2 Nonane, 4,5 dimethyl- 156 C11H24 017302-23-7 7 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 4 4 2-Acetylthiazole 127 C5H5NOS 024295-03-2 4 Abundance Scan 294 (7.741 min): 30015.D (-) m/z 4 .00 100.00% 43

5000

TIT" r' ' P 36 , 1 53 61 69.... 83.... 97 TITTHT ‘TT ‘TT‘ pi.. ।.... । rri. ।. । TIItrIrrTT r ■' ■ i 117122 7.40 m/z 124.85 7.60 7.80 8.00 9.49% m/z-? 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

— 5000 7.40 7.60 7.80 8.00 15 m/ z 46.85 7.70% I 35 85 97 117 125 ''11 ■ TTPI ITT ' 11 1 1 TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #11612; Nonane, 4.5-dimethyl- 43 5.7 MWKAW WAN 71 7.40 7.60 7.80 8.00 5000 - 85 m/z 96.95 6.82% l I I ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■'' P ■ ■ ■ i ■ ■ ■ ■ I ■ r 99 I • J ■ I ' • l ‘ 113 126 156 miz-> 10 20 30 40 50 60 70 80 90 100 11 120 130 140 150 160 Abundance #4732: N-Acetylpyrrolidone 43 7.40 7.60 7.80 8.00 m/z 82.95 6.16% 5000 - 99 127 56 86 . ...................................................... 30 - m/z~> 10 20 30 40 50 60 6970...80—90...— 112 ' i ■ ■' ■ i'1111'1 ■ ■ 11 ■ ■ ■ i ■ ■ ■ ■ i ■' 100 110 120 130 140 150 160 7.40 7.60 7.80 8.00

30015.D GCMS1126.M Tue Jan 15 15:37:49 2002 Page 2

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