GCMS analysis results for sample AD30015, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\30015.D Vial: 12 Acq On : 19 Dec 2001 2:50 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.42 ug/1 946202 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl form;amide 73 C3H7NO 000627-45-2 9 2 Silane, t ramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dio: olane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1,3-Diq olane, 2-methyl- 88 C4H802 000497-26-7 7 Abundance Scan 279 (7.603 min): 30015.D (-) m/ z 73.0.0 100.00% 73

5000- 43

87 103 7.20 7.40 7.60 7.80 8.00 37, |, 1 50 55 00 67, । ■ ■ i ■ ■ ■ • i ■ ■ • • l ■ ■ • TTttr । । TTn । । । TTT m/ z 43.0.5 28.52% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

5000- 58 7.20 7.40 7.60 7.80 8.00 44 m/ z 45.0,5 10.82% 15 ■ ■ i ' ■ ■ ' i 1 J ------- TONII, . . . r l . . <-T-J-TT-n-| I I I S | f I m/z-> 10 -20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73 TI—ur—num—mmr 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.05 10.38% 45 15 53 59 88 i • ■ ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । < • • • । ................................................ ... ■ ■ ■ ■ । TUUII । i । । । । । m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet TTIrr ITPmp—o TPTT r 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.0,0 7.02% 5000-

45

361 55 67 ' ' i ' ' ■ ' I 1 ' ' ' i ' ' 1 ' i ■ • 1 1 ...............I............... i ' + ■ l ■ • ■ ’ l -Irrnn tt-109 115 t7-T-r-n-p-r m/z-> 7.20 ′ 7.40 7.60 7.80 8.00 10 20 30 40 50 60 70 80 90 100 110 120

30015.D GCMS1126.M Tue Jan 15 15:37:43 2002 Page 1

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