GCMS analysis results for sample AD30013, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\30013.D Vial: 8 Acq On : 18 Dec 2001 10:55 pm Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.54 ug/1 897180 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dioxo ne, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Butane, 2 -methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 279 (7.603 min): 30013.D (-) m/ z 73.00 100.00% 73

5000 43 87 103 7.20 7.40 7.60 7.80 8.00 37, |, | 50 55 .61 67, । TIT I • ■ i ' • i ■ ■ > • । ■’> ■ r TIIIT । i m/z 43.05 27.78% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

5000- 44 58 7.20 7.40 7.60 7.80 8.00 m/z 41.0.5 10.82% 415 —4 1 i 1 1 r-j-, ■ ■ ■ i Tk" । । i > । > । i miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73 TnT I , , , Tr l I I I I 7.20 7.40 7.60 7.80 8.00 5000 m/z 44.95 10.19% 45 15 » 1 i • > > ■ | 53 59 ................................................ ................... । 88 । , |-|-|-|-i | i , | | | r miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet -Ti-r-r 73 7.20 7.40 7.60 7.80 8.00' m/ z 71.00 6.00% 5000-

45 ................. 3611 ' ■ i ' ' ' ■ i ' ■ ' ' i ' ' 1 ■ i ■ ■ ■ ' i ' ‘ 55 67. > i > ■ • > i ■ + ........ 109,115 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 ' 7.60 7.808.00

30013.D GCMS1126.M Tue Jan 15 15:34:17 2002 Page 1

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