GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\30254.D Vial: 12 Acq On : 22 Dec 2001 5:34 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 4.38 ug/1 1224060 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 000627-45-2 9 73 C3H7NO 2 Silane, tetramethyl- 000075-76-3 9 88 C4H12Si 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Butane/ 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 279 (7.607 min): 30254.D (-) m/z 73.00 100.00% 73

5000 43 . 7 ...

miz-> Abundance 10 20 37, |, | TTIPPTOITTITTTT TIB"—— * 1 1 I 1 r1'' 1141* 30 40 50 55 .61 67, । , 60 70 #292: N-Ethylformamide 80 87 90 100 103 110 120 m/z "T 7.20 7.40 7.60 7.80 8.00

30 73

5000 58 7.20 7.40 7.60 7.80 8.00 44 m/z 44.95 10.99% 15 mT -• i • * 1aaaa411**I* miz-> 10 20 30 40 150 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73 ........................... 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.00 10.61%

45 15 53 59 88 II—B—OTITT . . I i l ■ 1 I'11'I•'।।1■■■i1■■■ i ■ ■ ' ■ i ■ ■ ■ • i ■ ■ • • i ■ • m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet ==TTrmnTgEmuamT 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.56% 5000 45 36 55 - — ———————————————— 1 i ■ I 1 ' * i * <' • ' । 1 * 67, 109115 ' 111 ■ H ■ i ■ ■ ■ • i ■ ■ • ■ i ■ ■ • ■ i ■ ■ • ■ I • • m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

30254.D GCMS1126.M Wed Jan 02 10:15:17 2002 Page 1

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