GCMS sample analysis AD29235, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29294.D Vial: 10 Acq On : 12 Dec 2001 8:30 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.67 ug/1 166712 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-nt^thoxy-l-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2-(2/hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 3 2-Propanol, 1,1-oxybis- 134 C6H14O3 000110-98-5 50 4 2-Butanol, 3,3 -oxybis- 162 C8H18O3 054305-61-2 50 'Abundance 7 Scan 686 (11.341 min): 29294.D (-) m/ z 59.05 100.00% 59

5000

39 । r 45

51 73 103

11.00 11.20 ill 11.40 11.60 m/z-> ...... 30 40 50 --- 60 70 - 80 85- 90 — 110TT 120 .. 100 130 m/z 45.05 52.01% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 —IIT —T j — 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 35.12% -P - । । 111 । 130 ■ ■ i • ■ ■ ■ i » ■ > > i > ■ m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 , —T , TIT 11.00 11.20 11.40 11.60 5000- m/z 73.00 J 27.30% 31 45 103

it ......... .............. 75........... 89 ■ । ■ ■ ■ ' । ■ m/z--> 30 40 50 60 70 80 90 100 110 120 130 'Abundance #6087: 2-Propanol, 1,1’-oxybis- I—r Trm—mn I 1 1 1 1 I 59 11.00i 11.20 11.40 11.60 m/z 41.05 35 25.34% 31

NA 5000 45 103 — 89 72 I TPH-— • I 1 ’ ' ' j ’ ‘ 1 1 I 1 1 ' 1 I TT 1 i 1 ■ • r iT *1 1 r*-1 ' * i TUUIT m/z-> 30 40 50 I60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

29294.D GCMS1126.M Wed Dec 19 12:55:51 2001 Page 3

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