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GCMS analysis results sample AD29297, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036380–000036390

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29297.D Vial: 23 Acq On : 13 Dec 2001 12:26 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.78 ug/1 199353 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-2-methoxy-1-methylet 148 C7H1603 020324-32-7 72 2 1-Propanol, 2-(2-hydroxypropoxy) - 134 C6H14O3 .000106-62-7 53 3 2-Butanol, , 3 1 -oxybis- 162 C8H18O3 054305-61-2 50 4 2-Propanol, 1-(2-ethoxypropoxy)- 162 C8H18O3 010143-32-5 40 Abundance ' Scan 686 (11.339 min): 29297.D (-) m/ z 59.05 100.00% 59

miz-> 5000

20 ■ i • ■ ■ ■ i • 30 --51—44.. 40 45

50 60 80 84 73

TH PI- - j 1 1 I I I I I . I I I I t I I » 70 90 100 110 120 130 140 103

11.00 m/ z TT 11.20 11.40 11.60 45.05 NN ! -r-r-r-j-

48.36% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000- ■ । ■ ' • ■ । 45 103 11.00 11.20 11.40 11.60 73 31 m/z 102.95 35.33% TP ' I ' ' ' 1 I ' 0 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59

11.00 11.20 11.40 11.60 5000- m/z 73.00 ____ - 25.62%

NA 31 45 103

I h l_______ /_______ 75 89 ' i 1 ' ■ ' i ' ' i ■ ■ ■ ' i ' ' ■ ' I ■ ' ' ' i ' ■ ■ ■ i ■ ■ ■ ■ i ■ • ' ■ i-' ■ ■ ■ i ■ ‘ ■ i ■ ■ • ■ i ■ ■ 1 ■ j ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59 11.00 11.20 1140 11.60 m/z 41.00 23.84% 5000- 31 45 103

........... 134. - +— । , 11 ■ ■' ■ ।1'' ■ ।' ■ ■ ■ । ■ ■ ■ ■ । ■ - m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29297.D GCMS1126.M Fri Dec 21 12:19:44 2001 Page 2

NYC-WTC_000036388

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NYC-WTC_000036388Source: NYC Law Department, mirrored locally

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