GCMS sample analysis AD29235, Dec 2001

NYC 9/11 Public Portal Document

.Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29294.D Vial: 10 Acq On : 12 Dec 2001 8:30 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.65 ug/1 161833 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative / ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 23 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 1-Hexadecanol/ 242 C16H340 036653-82-4 9 4 1-Octadecano] 270 C18H380 000112-92-5 9 Abundance Scan 294 (7.743 min): 29294.D (-) m/ z 4 .95 100.00% 43

5000-

TT 63 83 97 125 7.40 7.60 7.80 8.00 - + —P "I' ........... -----.................. m/z 124.8,5 9.52% m/z-> 20 40' 60 80 100 120 140 160 180 200 220 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 TI 7.40 7.60 7.80 8.00 15 m/ z 82.95 6.33% ,85 97 125 miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #4732: N-Acetylpyrrolidone 43 DAA —A-AA 7.40 7.60 7.80 8.00 5000- m/z 126.90 6.32% 99 127 86 30 56 69 HI . 112 m/z-> 20 40 60 80 100 120 140__ 160 . 180 200 220 Abundance 43 #71247: 1-Hexadecanol 7.40 7.60 —A 7.80 ■ ■ । > ■ > • । 8.00 55 m/ z 96.95 6.17% 5000 83 27 70 97 111 | |, 125 .196 224 1 i ' ■ ■ ■ i ! r-p-r ■ ■ ।1 " I > ■ 1 • i ■'...................... ... । i । > । ■ । । i ■ "‘111.T r-j-r-r-r-r-j-, > i i | i , i , । m/z-> 20 40 60 80 100 120 140 160 180 200 220 7,40 7.60 7.80 8.00

29294.D GCMS1126.M Wed Dec 19 12:55:46 2001 Page 2

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