GCMS analysis results for sample AD30014, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\DEC18 0130014.D Vial: 13 Acq On : 19 Dec 2001 3:48 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.67 ug/1 177193 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1/1,1-trichloro- 160 C3H3C130 000918-00-3 39 2 Ethanol, 2,2,2 -trichloro- 148 C2H3C130 000115-20-8 9 3 N-Acetylpyrrolidone 127 C6H9NO2 . 000932-17-2 5 4 Dimethylpnosphinic azide 119 C2H6N30P 058347-13-0 4 Abundance Scan 294 (7.745 min): 30014.D (-) m/z 43.05 100.00% 43

5000

I-1 7.40 7.60 7.80 00 -351 +29. 74.2. .. ...... m/z 124.8,5 12.36% m/z->10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000- I-1 7.40 7.60 7.80 00 15 m/z 82.85 7.97% 1 35 85 97 117 125 I .... 1 .... j ■' • i ■ I • ■ ■' i ■ • ‘' i' ■ ■ ■ i ■ |'' ■ i ■ IT 1, I,. 1. ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66530: Ethanol, 2,2,2-trichloro- 31 AAA. A IA, 7,40 7.60 7.80 ' ' I ' 1 '• ■ i ■ 8.00 5000- m/z 126.90 6.99% 49 77 | 84 95 113 121 150 m/z--> Abundance 10 20 30 40 43 50 60 70__ 80__ 90 100 110 120 130 140 150 #4732: N-Acetylpyrrolidone 7.40 7.60 4 7.80 8.00 m/z 96.9,5 6.88% 5000- 99 127 56 86 30 69 ’ Ttrr1111111—111TCTTTTTTTI-ETTTT —..100 11?.. ..110 ..... j.... • I ■ ' ' I UI III I m/z-> 10 20 30 40 50 60 70 80 90 120 130 140 150 7.40 7.60 7.80 8.00

30014.D GCMS1126.M Tue Jan 15 15:36:08 2002 Page 2

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