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GCMS analysis results for sample AD30014, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report documenting analysis of sample AD30014 conducted on January 28, 2002.

NYC-WTC_000037301–000037313

Folder label: “GCMS X 12/11/01 A 12/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\30014.D Vial: 13 Acq On : 19 Dec 2001 3:48 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Anthracene-d10- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

25.12 0.26 ug/1 87504 Phenanthrene-dl0 24.98

Hit# of 5 . Tentative ID MW MolForm CAS# Qual

1 Anthr ene-d10- 188 C14D10 001719-06-8 78 2 4-Met yl-2-(3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 53 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 53 ( 4X~Methyl-2-(4-fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 53 \ Abundance Scan 2187 (25.123 min): 30014.D (-) m/z 188.10 100.00% 1(18

5000-

41 51 66 80 . 94| 160 24.80 25.00 25.20 25.40 136 । -------- +1............ —p ■ । ■ h‘I -.... . m/z 189.10 13.61% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000- 1 24.80 25.00 25.20 25.40 m/z 184.05 13.56% 66 80 9 160 i ! mmmm PPP i i । ri i i । —H | . . . . । . . m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 'Abundance #19859: 4-Methyl-2-(3-fluorophenyl)pyrimidine 188

24.80 25.00 25.20 25.40 5000- 121 m/z 187.10 13.56%

67 173 94 146 161 | 1 75 111. i [ > 11. r.. >. ।. 11 1111 > 111 v 111.1111 TTTITTT ‘ . । i-ii TT n 111 i*i 11 111 I' " ' I m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 24.80 25.00 25.20 25.40 m/z 94.00 12.82% 5000 102 115 145 I 51 63 75 94 130 158 TTIIWNIU "II' — ■ i' ■' ■ i ■ •'11 ■ ' ■ ■ i ■ PP 1___ i■"■i miz- > 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.80 25.00 25.20 2540 ' ' 1

30014 .D GCMS1126.M Tue Jan 15 15:36:22 2002 Page 5

NYC-WTC_000037312

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NYC-WTC_000037312Source: NYC Law Department, mirrored locally

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