GCMS analysis results for sample AD31462, Feb 11, 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31462 conducted on February 11, 2002.

NYC-WTC_000016320–000016329

Folder label: “GCMS X 12/28/01 A 1/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31462.D Vial: 27 Acq On : 17 Jan 2002 2:02 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

24.93 0.24 ug/1 74461 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene- 0- 001719-06-8 87 188 C14D10 2 Antipyrine 000060-80-0 53 188 C11H12N2O 3 Phenanthr .e-diO 188 C14D10 001517-22-2 50 4 4-Methyl -(4-fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 42 Abundance Scan 2166 (24.926 min):31462.D (-) “ “ ~Tm/z 188.10 100.00% 188

5000 .......... / \............................ . . , i , r i p i r i । । । । । । । । . । । 80 94 . 24.60 24.80 25.00 25.20 36 44 52 66 | 132 160 rr-p- m/z 94.00 16.16% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-dlO- 188

5000 24.60 24.80 25.00 25.20 ' ' ‘ _ 80 m/z 79.95 13.64% 66 1 160 : III T| n 11 । 11111 1111 । i > i 111 i i I | i । । 11 11 i । । ril, 111 . i. • । ■ i" ■ • 11 • i ■. । ■ i • ■ ■ ■ | • miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 119872 Aotnypina 188 96 24.60 24.80 25.00 25.20 5000 77 m/z 189.05 13.23% 56 105 ................ 1....... ‘ 159 173 “ i “ “ i ‘‘ i ■ " ‘ i ■ ■ " i “ ■ ■ i' ■ ■ ‘ i “ " i “ ‘11 • miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 ‘ ‘ I ‘ ' I1 ' 1 ■ I 1 1 1 1 1 1 1 ‘ 1 1 188 24.60 24.80 25.00 25.20 m/z 184.10 11.39% 5000

160 1mTpmpTTTT 66 80 94 1111111111111111111111111111111 rrrm i'I'I 11111 * 1 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20

31462.D GCMS0103.M Thu Feb 07 12:39:52 2002 Page 2

NYC-WTC_000016328

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