GCMS analysis results for sample AD31255, Feb 25, 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31255 conducted on February 25, 2002.

NYC-WTC_000016423–000016441

Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02”

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NYC 9/11 Public Portal Document

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Data File C: \HPCHEM\ 1 \DATA\JANO 802\31255.D Vial: 9 Acq On 9 Jan 2002 9:35 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

24.95 0.23 ug/1 81081 Phenanthrene-dl0 24.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene -010 188 C14D10 001719-06-8 90 2 4-Methyl-2/ (3-fluorophenyl )pyrimidi 188 C11H9FN2 076128-66-0 45 3 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 4 Phenanthrene -diO 188 C14D10 001517-22-2 38 Abundance Scan 2168 (24.949 min): 31255.D (-) m/z 188.10 100.00% 188

5000 ■ ■ i ■ ■ • i i • ■ ■ ■ j • ■ ■ ■ i ■

43 52 69 80 94 108 132 160 24.60 24.80 25.00 25.20 —hmhhhmmmmmmpmg .w. m/z 94.05 14.06% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d IQ- 188

5000 24.60 24.80 25.00 25.20 ' ' H m/z 80.05 13.60% 66 80 9 i" ............... ।।I.।1111■11111111111111111111111111111.111.।i11,1111111111 T’T 160 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #10352. -Methy-2-(3-fluorophenyl lpyrimidine 188

24.60 24.80 25.00 25.20 5000 121 m/z 184.10 12.51% 1 67 173 94 1 75 146 161 | | i" “ i ■ • ■ ■ i “' ■ i “ ■11 ‘1 ■' i ■ ■" i11" 11111111'11'"111"1111 •1 ■ i ■ ‘11 i11111 •1 ■11 ■ ■ • ■ i ■ ■ m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165:2-Quinolinecarboxaldehyde, 8-hydroxy- oxime 188 24.60 24.80 25.00 25.20 ' m/z 189.10 11.99% 5000 143 89 64 I I | 1 I I I130 । 1 I ।116 158 170 h I | I mmmp mmTDTTTT |'l I . I | II, 1’8 L miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 180 170 180 190 24.60 24.80 25'ob 25.20 ‘

31255.D GCMS0103.M Wed Feb 06 11:23:45 2002 Page 3

NYC-WTC_000016432

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NYC-WTC_000016432Source: NYC Law Department, mirrored locally

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NYC-WTC_000016442

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