GCMS analysis results for sample AD31364, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31364 .D Vial: 16 Acq On : 17 Jan 2002 2:18 am Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

24.92 0.25 ug/1 75934 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene- 2=9 2 2-Quinoline carboxaldehyde, 8-hydrox 188 C10H8N2O2 001719-06-8 78 005603-22-5 40 188 C14D10

3 3-Quinolinecarbonitrile, 1,2,3,4-te 188 C10H8N2O2 022384-05-0 40 4 5-Oxazolecarboxamidez 2-phenyl- 188 C10H8N2O2 039819-42-6 40 Abundance Scan 2165 (24.923 min): 31364.D (-) m/z 18.8.10 100.00% 188

5000 1d.n//t/t////501/2/1/0/02/B/B/n"T 41 54 64 80 94 132 146 160 24.60 24.80 25.00 25.20 111-HHmmHTP m/z 185.10 15.70% 40 50 60 70. 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 ----- 24.60 24.80 25.00 25.20 80 94 m/z 184.10 13.39% 66 160 1111 Mmmmmmmmmpr ■ ■ i • ■ ‘ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • T’T miz-> 40 50 60 70 80 90 100 110.120 130 140 150 160 170 180 190 Abundance - ■ Gnch f cobowaldohyk 8-hyury- oxime 188 . . । । i . r . 1 i i । । । । । । i । 24.60 24.80 25.00 25.20 5000 m/z 94.00 11.77% 143 89 115 130 h 158 170 ■ ■ i ■ ■ ‘' i " ■ ■ i1 “ ■ I ■ • “ i ‘" i ■ ■ “ i " ■ ■ i " 1 ■ i “ ■' i “ " i11'111 ■ ‘ ■ i'' ■ ■ i1 ' i ■ ■ ■11 ■ ‘ ■ m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .................. ....................... Abundance #19815:3-Quinolinecarbonitrile, 1,2,3,4-tetrahydro-1-hydro 188 24.60 24.80 25.00 25.20 m/z 80.00 8.89% 128 172 5000 93 117 142 66 I - '1'11''1' 111 • ‘ 11' I “ ‘ • I ‘11 ‘ n * 1 “ ’ 1’3 rp-r miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20

31364.D GCMS0103.M Thu Feb 07 09:12:24 2002 Page 2

NYC-WTC_000018332