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GCMS unknown compounds report, sample AD31363, Feb 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP sample AD31363 identifying unknown compounds and surrogate recovery results from February 13, 2002.

NYC-WTC_000016514–000016523

Folder label: “GCMS X 12/31/01 A 1/18/02

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Scanned page image, NYC-WTC_000016522
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31363.D Vial: 8 Acq On : 16 Jan 2002 6:29 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

24.92 0.24 ug/1 70232 Phenanthrene-dl0 24.77

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracen,d1057 188 C14D10 001719-06-8 91 2 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 38 3 Phenanthrene-diO 188 C14D10 001517-22-2 38 4 5-Oxazolecarboxamide, 2-phenyl- 188 C10H8N2O2 039819-42-6 38 Abundance. 7 ~~ Scan 2165 (24.918 min): 31363.D (-) m/z 188.10 100.00% 188

5000

94 • ■ । • p ' 1 ■ i ■ • ■ ■ । • ■ ■ ■ । 160 ,

m/z-> 66 80 40 52 - II—,pt 30 40 50 102 +24++ 60 70 80 90 100 110 120 130 140 150 160 170 180 190 •p-n- 24.60 24.80 25.00 25.20 m/z 94.00 17.66% Abundance #19957: Anthracene-d 10- 188

5000 ■ ‘ | ■ r ■ p ■ r • l . • ■ • I ■ ■ • ■ | 24.60 24.80 25.00 25.20 m/z 184.10 15.67% 66 894 .ii° -WTmTTTTTWWWmPTTT | miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19306 : Qurrolmecarboxaldchyde. 3-nydroxy- oxint 188

24.60 24.80 25.00 25.20 5000 m/z 189.10 15.37 . 115 143 89 130 158 170 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 24.60 24.80 25.00 25.20 m/z 160.05 11.219 5000

66 80 94 160 | mmmmmmmmmmmmmmmmmmmmmmmmmm ■n j-t i n |T i t i । i i i i । i n Tg miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20

31363.D GCMS0103.M Thu Feb 07 09:11:31 2002 Page 2 NYC-WTC_000016522

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NYC-WTC_000016522Source: NYC Law Department, mirrored locally

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