GCMS analysis results for sample AD31255, Feb 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\1\DATA\JAN0802\31255.D Vial: 9 Acq On 9 Jan 2002 9:35 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.61 0.67 ug/1 182020 1,4-Dichiorobenzene-d4 11.53

Hit# of 5 Tentative ID MW Mol Form CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 56 2 3-Pentyn-2-one, 5,5-diethoxy- 170 C9H14O3 055402-04-5 9 3 1 - Oc t adecano 1 270 C18H380 000112-92-5 7 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 Abundance Scan 279 (7.608 min): 31255.D (-) m/z 4 .00 100.00% 43

5000

I"1"'1'r | * 1 * * । * * < * । i * * * । i i 9 83 97 125 7.20 7.40 7.60 7.80 8.00 ; 1,110002 I-, , .9.? " 207 , ........ m/z 124.85 9.80% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

i * ■ ■ ■ i ‘ * i M,-i p 5000 7.20 7.40 7.60 7.80 8.00 15 m/z 96.85 7.90% 85 97 125 PTTH ' I ‘ ‘ ‘ ' l 1 • ' ’1 • • • 1 ihi ■ ■ | ■ i i i | ri i i | r i i i । r i i i । i i i i । . i i i ! m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #15121; 3-Pentyn-2-one. 5.5-diethoxy- 43 1**1** ■ • i ■ ■ ■ • i ■ ■ 7.20 7.40 7.60 7.80 8.00 5000 55 m/z 82.9.5 7.43% 83 97 69 83 125 .../ 111 ..... . miz-> Abundance 20 40 43 60 80 100 120 140 160 #72027: 1-Octadecanol 180 200 220 240 260 MA.A.M.A 7.20 7.40 7.60 7.80 8.00 m/z 81.85 6.45% 5000 82 56 68 97

■ ■ i ■ ■ ■ ■ ।1 ‘11 | 111 125 1122/0/11/0/0/n/TT0[o ——u—;1un—,——Tg—3—t 224 270 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 7.20 7.40 7.60 7.80 8.00

31255.D GCMS0103.M Wed Feb 06 11:23:41 2002 Page 2

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