GCMS analysis results for sample AD31642, February 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\JAN0302\31642.D Vial: 33 Acq On 4 Jan 2002 5:42 pm Operator: 209 GALOS Sample gems scan 1/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.61 0.72 ug/1 152173 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 38 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 1-Octadecanol 270 C18H380 000112-92-5 9 4 2-Acetylthiazole ____________ 127 C5H5NOS 024295-03-2 7 Abundance Scan 279 (7.609 min): 31642.D (-) m/z 43.05 100.00% 43

5000

Un p 4111 iiT-rj! MPr 63 82 97 125 7.20 7.40 7.60 7.80 8.00 BIIUn’t V,.... h I................. . m/z 124.85 14.10% mlz-? 20 40 60 80 100 120 140 160 180 ‘266 220 240 260 Abundance #12247:2-Propanone, 1,1,1-trichloro- 413

......... . 5000 7.20 7.40 7.60 7.80 8.00 15 m/z 46.85 8.32% 11 ■ ।. . > ‘1 । '1 'r 11 11 .85.97 ........................................... miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance 43 #4732: N-Acetylpyrrolidone WwMWWut 7.20 7.40 7.60' 7.80 8.00 5000 m/z 81.8,5 7.94% 99 127 86 30 । . 56 69 112 • ■ i ■ ■ • ■ 1 • • ' * i ■ ■ ■ ■ i 1’1 •■i■■■•i■■■11'■‘‘l1<■*।1 • * ■ i'11111 *111 * mfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #72027:1-Octadecanol । / 11 i । » J • » { 1 1'| 11 i" 1 j r 1 43 7.20 7.40 7.60 7.80 8.00 m/z 96.8,5 7.31% 5000 82 56 68 97

• • । • • • ■ । —L 1111125.... .0222 J I I I I”I * » » >1 I > » « I i'll' J J kT m/z—> 20 40 60 80 100 120 140' 160 180 200 220' 240 260 7.20 7.40 7.60 7.80 8.00

31642.D GCMS1126.M Fri Feb 01 11:18:26 2002 Page 2 NYC-WTC_000049742