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GCMS analysis results for sample AD29670, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036842–000036859

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036850
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0302\29670.D Vial: 15 Acq On 4 Jan 2002 12:13 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

7.61 0.54 ug/1 258300 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130> 000918-00-3 40 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 Ethene, chloro- 62 C2H3C1 000075-01-4 9 4 2-Acetylthiazole____________________ 127 C5H5NOS 024295-03-2 7 Abundance ■ 2 Scan 279 (7.609 min): 29670.D (-) m/z 43.05 100.00% ’ 43

5000- Tpor r TPPPTmgT 35 ,49 61 72 63 97 119125 7.20 7.40 7.60 7.80 8.00 IT TITT I I1!1! II I 1t‘r I I | I I I I | I1!1! I | I I TI I I I | I I TrTr T m/z 124.95 9.54% mlz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 48

5000- ---------- 7.20 7.40 7.60 7.80 8.00 15 m/z 82.95 6.16% I TIT 35 49 85 97 117 125 -trrrr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone 43 .......................................................... 7.20 7.40 7.60 7.80 8.00 5000- m/z 126.90 5.89% 99 127 56 86 3 I • i ■ • • • i • 69 ■ । • ■ ■ • । li ■ . 112 I m/z-> 10 20 30 40 50 60 70 80 !90 100 110 120 130 Abundance #135: Ethene, chloro- 27 7.20 7.40 7.60 7.80 8.00- 62 m/z 96.95 5.84%

5000-

35 'I ' ' • ' I * ' I i. 4450 —60 111 ■1 ■ i' ' ' I ' ' ■ ' i ' ' ' ' i ' ' ' ■ i 1 ' 1 ' i ' ' ' ' i ' ' ' ■ i ' ' miz-> 10 20 30 40 70 80 90 100 110 120 130 1 7.20 7.40 7.60 7.80 8.00

29670.D GCMS1126.M Wed Jan 16 14:50:33 2002 Page 2

NYC-WTC_000036850

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NYC-WTC_000036850Source: NYC Law Department, mirrored locally

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