GCMS analysis results for sample AD29670, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0302\29670.D Vial: 15 Acq On 4 Jan 2002 12:13 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. -EstConc Area Relative to ISTD R.T.

7.47 3.03 ug/1 1444090 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3 -Dioxolane , 2-methyl- 88 C4H802 000497-26-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane, 3-methoxy­ 102 C6H140 _______ 036839-67-5 9 Abundance ' ' Scan 264 (7.471 min): 29670.D (-) m/z 73.00 100.00% 73

5000 43

7.20 7.40 7.60 7.80 0- ........... 381 ,| 50 55,60 67 i 1IT — — 87 103 ————— m/ Z 43.00 32.88% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73

5000 43 T—IB—B—B—n/I—r 7.20 7.40 7.60 7.80 58 m/z 45.05 ‘ 11.54% 87

m/z-> i 10 ■ • ■ ■ i 20 4l—. 4. 30 40 50 60 I ■ ■ ■ • l . i 70 —————————————— 80 90 ( : > T-r-f-r-i 100 110 Abundance #292: N-Ethylformamide 30 73 TTn.uuu 7.20 7.40 7.60 7.80 . 5000 m/z 41.05i 11.40% 44 58

15 > ■ i ■ • ■ ■ । —I ' ' ' ■ i ' ' ' ' i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- — 73 7.20 7.40 7.60 7.80 m/z 71.00 6.89%

miz—> 5000

15 i ■ ■ ■ ■ l 10 20 31 | 55 45 ------ I । —————— 30 40 50 60 70 I ————— 80 88 90 । i m-r-p 1 100 110 7.20 £ 7.40 7.60 7.80

29670.D GCMS1126.M Wed Jan 16 14:50:28 2002 Page 1

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