GCMS sample analysis report with surrogate recovery, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC1401\29926.D Vial: 45 Acq On 16 Dec 2001 9:40 am Operator: 209 GALOS Sample gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.66 ug/1 170792 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, /l,1,1-trichloro- 160 C3H3C130 000918-00-3 39 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 2-Propanone, 1,1-dichloro- 126 C3H4C12O 000513-88-2 9 4 2-Acetyl/l,4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 4 Abundance Scan 293 (7.737 min): 29926.D (-) m/ z 42.95 100.00% 43

5000-

1 1 1 11 1 ' I ' 1 ■ • । • ■ > • । • ■ • • । 53 61 72 82 97 119125 7.40 7.60 7.80 8.00______ 37 J r-m-r ‘ t TTTTTT-TTIIPPTPTTTT m/z 124.85 7.76% m/z-> 10 20 30 ■ 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 -0rt""d 7.40 7.60 7.80 8.00 15 m/z 96.9 5 6.53% I 35 49 85 97 117 125 • ' ' i ' m/z-> 10 20 30 40 50 60 70 80 90 100 11 120 130 Abundance #4732: N-Acetylpyrrolidone 43

7.40 7.60 7.80 8.00 5000- m/z 126.90 6.52% 99 127 56 86 30 , . . p . , ,. । , ttrrTT p III 69 112 ■ । ■ • • • । • m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4368: 2-Propanone, 1,1-dichloro- ■ i ' ■ ■ ■ i ' ' ' ' i 48 7.40 7.60 7.80 8.00 m/ z 81.8.5 6.32% 5000-

15 27 TUT m • y-r-m-p-m p 37 , 49. 6376 83 .......... --- m/z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.60 7.80 8.00

29926.D GCMS1126.M Wed Jan 30 11:50:26 2002 Page 2

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