GCMS analysis results for sample AD30486, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30486.D Vial: 21 Acq On 1 Jan 2002 6:23 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.75 0.58 ug/1 153738 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 - Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 38 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 3 2-Acetylthiazole 127 C5H5NOS 024295-03-2 4 4 3-Pentyn-2-one, 5,5-diethoxy~ 170 C9H14O3 055402-04-5 4 Abundance 43 Scan 295 (7.749 mln): 30486.D (-) m/z 43.05 100.00%

5000

35 ■ ■ i ■ ■ ■ ■ । ■

—।— । i 1dy | | | t । i 150 .. 61 Jr., ill 150 | I I | | | I I > I । । । । । । । । । । ,85 97 ; r( । । 117 125 | 1 i v 1 | * i 4‛a‛y * I I I 7.40 m/z 7.60 35.00 7.80 8.00 13.95% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 7.40 7.60 7.80 8.00 15 m/z 124.85 11.22% | 35 49 85 97 117 125 1 ■ i ■ ' • ■ i ■ • ■ ■ i ■ ■ ' • i ■ * • t'J I <11 J 1 rrrgi I 1 I I I I*J 1 11 ■ ■11 • • • ■ i • • ■ ''i'' >' i । ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone 43 T V 7.40 7.60 7.80 8.00 5000 m/z 126.90 10.62% 99 127 30 56 86 69 । • • j > > I > *»1111» ■ i ■ ■ ■ ■ i •1 ’' i‘1' ’11''' ii1 1IY i | • i i i.n । T 1 I I 112 | I 'I I ! | J I I I | ) ! m/z-> 10 20 30 40 50 60 70 80> 90 100 110 120 130 Abundance #4717:2-Acetylthiazole ***111IILi 43 7.40 7.60 7.80 8.00 m/z 46.90 10.11% 5000 58 85 99 112 127 WYhsMan"yoawob ‘ ■ I ’ ‘ 33 ' I 1 ' ' ' I ' ‘ ‘ ' I' ‘ ‘ • l • ’ I,.......... n....... 1 ■ i' ■ ■ ■ i ■ ■ ■ ■ i ‘ST‘T‘"l > 11 ■ m/z-> 10__ 20__ 30 40__ 50 60 70 80 90 100 110 120 130 7.40 - 7.60 7.80 8.00

30486.D GCMS1126.M Tue Jan 15 14:51:16 2002 Page 2

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