GCMS analysis results for sample AD30486, Jan 2002

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Laboratory report detailing GCMS analysis of sample AD30486 including DDD surrogates on January 18, 2002.

NYC-WTC_000017097–000017107

Folder label: “GCMS X 12/14/01 A 1/1/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\1\DATA\DEC3101\30486.D Vial: 21 Acq On 1 Jan 2002 6:23 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Undecene, 9-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

32.74 0.35 ug/1 76664 Chrysene-dl2 33.02

Hit# of 5 T ative ID MW MolForm CAS# Qual

1 1-Undece: , 9-methyl- 168 C12H24 074630-41-4 27 2 2-Unde ne, 9-methyl-, (E) - 168 C12H24 074630-46-9 27 3 2-Unj cene, 9-methyl-, (Z) - 168 C12H24 074630-45-8 27 4 Oc ne, 1/1'-oxybis- 242 C16H340 000629-82-3 27 Abunda Scan 3017 (32.738 min): 30486.D (-) m/z 56.95 100.00% 57 112 70 43 83 5000

97 239 256 m A, m, A AMY, MAnM

m/z-> ui ■ ■ rtf 20 40 60 I| li Hi • ■ i ‘ 80 4 129 I ’147*’1+11414/’1++11141**I’’-’14’’’: 100 120 140 160 180 200 220 240 260 J__ L 32.40 32.60 32.80 33.00 m/z 112.10 85.17% Abundance #14707:1-Undecene, 9-methyl- 55 70

83 5000 97 32.40 32.60 32.80 33.00 m/z 70.00 81.17% 111 139 168 1 । ■ ■ ■ ■ । ■ ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #14731 2-Undecere 9-methyl-, (E)

5000 55 70

83 A. 1 1 i 1 1 ■ • i 1 1 1 4 > ' 32.40 32.60 32.80 33.00 m/z 71.10 81.05% 97 27 42 139 168 I ' i ‘ ‘ ‘ i 1 ■ • • i 1 • ■ ■ i ‘ ' 1 'I ‘ ‘ i rl’ > । । > | > । > ■ i • • ■ ■ i ■ ■ 1 1 i ■ ' 1 1 i111111 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 A ■, AW, m AM’MAAA, Abundance #14730:2-Undecene, 9-methyl-, (Z)- 55 73 32.40 32.60 32.80 33.00

J m/z 55.0.0 74.75% 83 5000

i 27 | 42 i ■ • • • i ■ ■ II...... 139 168 (’d. 11*4/4 I j-1 » . I I l t I J ‘I J I J t ] > I I / | I I I : | > i > I j > > i I | I I ! I |"l A AMAAY, YW m/z-> 20 40 60 80 100_ 120 140 160 180 200 220 240 260 32.40 -32.60 32.80 33.00

30486.D GCMS1126.M Tue Jan 15 14:51:21 2002 Page 3

NYC-WTC_000017106

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