GCMS unknown compounds report, sample AD31251, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0802\31251.D Vial: 16 Acq On : 10 Jan 2002 4:26 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1-Decene, 2,4-dimethyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.42 1.08 ug/1 174257 Perylene-dl2 36.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Decene, 2,4-dimethyl- ,0 168 C12H24 055170-80-4 17 2 2-Undecene, 2,5-dimethyl- ) o 182 C13H26 049622-16-4 16 3 4 -Undecanol , 7 - ethyl - 2Ametkyi- 4 Nonante, 3-methyl-__________ E Abundance / Scan 3308 (35.416 8 31251 .D(-)

57 185 214 C14H30O 142 C10H22 m/z 50 000103-20-8 005911-04-6 12 10

5000 70 43 112 83 98 । • * • • i • • • • । • • • •Trr* • i * * TOT '1144,4 — 1125 139 166 ■‘i'■'■i'■■■i 203 268281 297 ।> i • * • ■ i •: > > f • • ■i • 35.00 35,20 35.40 35.60 35.80 m/z 57.00 69.52% mlz~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #14795: 1-Decene, 2,4-dimethyl- 48 57

83 5000 70 35.00 35.20 35.40 35.60 35.80 112

l m/z 70.10 47.18% 97 168 i ■ • ■ • i • • • ■ । • • • • । • ■ i' ■ • ■ i • • • • i ■ ■ ■ ■ i' ■ ■ ‘ i1 ■ • ‘ i' ‘ ‘ ‘ i ■ ■ ‘ ■ i ■ • ‘ ■ i ‘ ■ i ■ ■ ■ ■ i ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance - 1-489. 2-Undecone, 2.5-d methyl- 57 70 35.00 35.20 35.40 35.60 35.80 5000 m/ z 55.00 45.25%

27 42 j 83 , 182 97 111 126 I - m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #26416:4-Undecanol. 7-ethyl-2-methyl- MMAAMMMY , .

I 57 35.00 35.20 35.40 35.60 35.80 m/z 71.10 41.71% 5000 70 27 1 83 98 no : m/z-> 1.112125 4M I ' ‘‘ l ' ' 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 35.00 35.20 35.40 35.60 35.80

31251.D GCMS0103.M Wed Feb 06 11:19:57 2002 Page 5

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