GCMS unknown compounds report, sample AD31251, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0802\31251.D Vial: 16 Acq On : 10 Jan 2002 4:26 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.29 0.38 ug/1 110234 1,4-Dichlorobenzene-d4 11.53

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H1603 020324-32-7 64 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 3 Ethane, 1- ethoxy-1 - methoxy- 104 C5H12O2 010471-14-4 45 4 2-Butanol, 3,3’ -oxybis- 162 C8H18O3 054305-61-2 45 Abundance Scan 680 (11.290 min): 31251 .D (-) m/z 59.05 100.00% 59 45 5000 103 73 11.00 11.20 11.40 11.60 miz-> 4 ■ । • ■ ■ ■ । • 20 30 40 50 60 70 80 90 86 ‘ l 1 rl ‘‘l ‘ 100 110 । ' 1* , i । । i r | 120 i i . | > i 130 m/z 45,05 55.25%

NWA Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 11.00 11.20 11.40 11.60 73 31 m/z 103.00 34.99% : h।■1 . . । I Jr • i * • 130 | .... I > t-PPP ■ i ‘ ‘ ‘ i ' ■ • ‘ i ‘ • m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-4{2-hydraxypropoxy)- 59 IIOM ■ i ■ • • * i ■ ‘ ' i 1 ■ 11.00 11.20 11.40 11.60 5000 m/ z 41.05 31.84% 31 45 103

75 89 * I • • » >"1 ‘ i ‘ ‘ i • ' ■ • i • ' ■ ■ i 1 • ■ ■ i ' ' ' ' i ' 1 ■ ■ i ‘ ■ i ■ • • ■ i ‘ 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1926: Ethane, 1-ethoxy-1-methoxy- ATMTIumumpu—mm—rr 59 11.00 11.20 11.40 11.60 45 m/z 73.00 5.44% 5000 73 89 27 —PPT *ugrr 103 .............. ■ । * • •1111 ■ ■ । • ■ ■ ■ । • •' ■ । * •1111 ■1 ■ i' ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

31251.D GCMS0103.M Wed Feb 06 11:19:52 2002 Page 4

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