GCMS unknown compounds report, sample AD31251, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0802\31251.D Vial: 16 Acq On : 10 Jan 2002 4:26 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHQDS\GCMSO1O3.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

11.21 0.36 ug/1 103976 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol,1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 64 2 2-Pentano: e, 5-methoxy- 116 C6H1202 017429-04-8 45 3 1- Propano , 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 4 2 - Propaw1, 1,1'-[(l-methyl-l,2-eth 192 C9H20O4 001638-16-0 42 Abundance Scan 671 (11.207 min): 31251 .D (-) m/z 59.05 100.00% 59 45 5000 73 103

miz-> -1 30 39, 40 1 50 t 60 70 1I— 80 85TT 90 100 110 120 130 10.80 11.00 11.20 11.40 11.60 m/ z 45.05. L. 54.01% Abundance #9238:2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

5000 45 73 103 10.80 u'oo 11.20 11.40 11.60 31 m/z 102.95. 29.41%

miz-> -P 30 40 50 160 “ ■ 1 70 1' 1 m-j-r-r-r-r-p- 80 90 um 100 110 ■ i ■ • 1 ' I ‘ 120 130 ■ i ■ ‘ 130 Abundance #64282: 2-Pertanone 5-meinoxy- 43 59 10.80 11.00 11.20 11.40 11.60 ...... ................. 5000 m/z 41.05 27.46% j f 69 84 101 116 ‘ ' I ' ‘ ‘ ' I ‘ ‘ ‘ • | • ■ • ■ | ■ "L"Ii , , i । , , , , । , , , , । , i , । i r i , । i , i , । , miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086:1-Propanol, 2-(2-hydroxypropoxy)- 59 10.80 11.00 11.20 11.40 11.60 m/z 73.00 26.56% 5000

My 31 45 103

-PPPP------+H 75 89 ■ i ‘ 1 ■ ■ i ' ■ ' • i ■ ■ ■ • i ■ 1 • ■ i • 1 ' ‘ i • • • ■ i ■ ■ m/z-> 30 40 50 160 70 80 90 100 110 120 130 10*80 11.00 11.20 11.40 11.60

31251.D GCMS0103.M Wed Feb 06 11:19:47 2002 Page 3

NYC-WTC_000016470