GCMS analysis log for sample AD30696, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30696.D Vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

11.45 0.51 ug/1 129592 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 Ethane, 1 -ethosy-1-methoxy- 104 C5H1202 010471-14-4 50 3 2-Propanol , 1,1 ’ - oxybi s- 134 C6H14O3 000110-98-5 38 4 2-Pentanone, 5-methoxy- 116 C6H12O2 017429-04-8 33

N Abundance Scan 698 (11.450 mln): 30696.D (-) m/z 59.05 100.00% 59 45 5000 73 103

....... > 51 85 11.20 11.40 11.60 11.80 1 44

N— 1 1 I ' • । • i • m/z 45.00 57.26% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 11.20 11.40 11.60 11.80 ' 73 31 m/z 103.05 29.87%

miz-> Abundance

5000 ■ । 1 1 20 । 30 ।I • । *i • • 40

45 50 Tr 1"' ‘‘I 1 ' 1 ' i ' 11 ■ i1 i ' 110 120 130 60 59 70

73 80 90 100 41926; Ethane. 1 -ethoxy-1 -methoxy-

89 130

_M m/z 11.20 11.40 11.60 11.80 41.05 27.22%

miz-> Abundance 20 27

30 40 _________ _________ __________________ 103____________ ■ 1 ■ i ■ ■ ■ • i ■ • ■ ‘ i ■ • ■ • i •' ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i' ' 1 11 Tn/d 1 i 1 1 50 60 70 80 90 #6087:2-Propanol, 1,1’-oxybis- 59 100 110 120 130 MWMv NA 11.20 11.40 11.60 11.80 m/ Z 73.00 25.35%

A 31 5000 45 103

m/z-> 20 30 40 ^-■311!'...

50 60 72 89 T-I-r-r 1 1 i ■ 1 ‘ ■ I • • ■ ■ i ■ 1 ■ ■ i ■ ' 1 1 I 1 1 ' 1 I ' ' 70 80 90 100 110 120 130 N, 11.20 11.40 11.60 11.80

30696.D GCMS1126.M Wed Jan 23 08:36:41 2002 Page 3

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